(E)-1-(4-Chlorobenzylidene)thiosemicarbazide
نویسندگان
چکیده
منابع مشابه
Microwave assisted synthesis of [4, 5-e] [1, 3, 4]thia- diazin-7-yl] hydrazine Derivatives
New pyrimido [4, 5-e] [1, 3, 4]thia- diazin-7-yl] hydrazines were synthesized via the cyclocondensation of alkyl-2-phenylhydrazinecarbodithioates as a binucleophile with 5-bromo-2,4-dichloro-6-methylpyrimidine as a bielectrophile , and replacement of C-7 chloro atom by hydrazine in ethanol as the solvent . This method has advantages over methods currently described in the literature for the con...
متن کامل(E)-1-(4-Chlorobenzylidene)thiosemicarbazide
In the crystal of the title compound, C(8)H(8)ClN(3)S, mol-ecules are connected by N-H⋯S hydrogen bonds into strips parallel to the (112) planes and running along [10]. One of the amino H atoms is not involved in a classical hydrogen bond. In addition, there is a rather short inter-molecular Cl⋯S distance of 3.3814 (5) Å.
متن کامل4-[(E)-1-Naphthyldiazenyl]phenol
The title compound (C. I. Solvent Yellow 8), C(16)H(12)N(2)O, crystallizes with two crystallographically independent mol-ecules in the asymmetric unit. The planarity of both mol-ecules is slightly distorted, the dihedral angles between the benzene ring and the naphthalene system being 9.04 (8) and 5.69 (3)°. In the crystal, O-H⋯N hydrogen bonds between the hydr-oxy groups and azo N atoms link t...
متن کامل(E)-1-(4-Bromophenyl)-2-(4-tert-butylphenyl)-1-phenylethene
In the structure of the title compound, C(24)H(23)Br, the configuration about the double bond is E. The dihedral angles between the tert-butyl-substituted benzene ring and the unsubstituted and Br-substituted rings are 57.1 (2) and 78.2 (2)°, respectively. The methyl groups are disordered over two positions; the site occupancy factors are ca 0.8 and 0.2.
متن کامل(E)-1-[1-(4-Chlorophenyl)ethylidene]thiosemicarbazide
In the crystal structure of the title compound, C(9)H(10)ClN(3)S, the mol-ecules form chains parallel to [001] through N-H⋯S hydrogen bonds. In addition, weak inter-molecular N-H⋯Cl hydrogen bonds connect the chains, forming a two-dimensional network parallel to (001).
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2011
ISSN: 1600-5368
DOI: 10.1107/s1600536811004120